This research investigates comprehensive valorization of coconut powder waste, an abundant agricultural byproduct, for sustainable briquette fuel production through systematic process optimization. The study encompasses three primary objectives: optimization of coconut powder carbonization parameters, evaluation of coconut-palm residue blend ratios, and assessment of storage stability characteristics. Carbonization temperature significantly influenced charcoal quality, with optimal conditions achieved at 300 °C, yielding moisture content of 5.36% and exceptional fixed carbon content of 84.49%. Higher temperatures (320-360 °C) adversely affected fuel quality through increased ash and volatile content. The most favorable coconut charcoal-to-palm residue blend ratio of 50:50 demonstrated superior performance characteristics, including highest calorific value (5950 cal/g), optimal fixed carbon content (80.67%), and enhanced storage stability. Excessive palm residue proportions (75%) significantly compromised fuel quality, evidenced by elevated ash content (40.36%) and reduced fixed carbon (39.69%). Ultimate analysis revealed that the optimized 50:50 blend exhibited maximum carbon content (82.20%) and minimum oxygen content (8.46%), indicating superior combustion efficiency. Storage studies demonstrated excellent stability over 90 days with minimal moisture reabsorption and maintained structural integrity. The developed briquette fuel represents a viable sustainable energy solution, transforming agricultural waste into high-quality renewable fuel while addressing waste management and energy security challenges.